Oxygen in Aluminium

Power Mode:     Continuously

Sample Drop:     Automatic

Out-Gas Power (Kw)    4.2

Out-Gas Time (Sec)    30

Purge Time (Sec)     10

Stabilization Time (Sec)    45

Integration Delay (Sec)    5

Analyse Power (Kw)    3.2

Minimum Time (Sec)    25

Maximum Time (Sec)    60

Comparator Setting    20

Accelerator / Flux x2 Tin Pellets (AR 639)

Graphite Crucible x1 Outer Crucible (SL 433) + x1 Inner Crucible (SL 431)

Sample Preparation Sample weight approx. 250mg. Remove any surface oxidation by abrading. Ensure the sample is clean.
 

  

Nitrogen in Boron Nitride Ceramics

Power Mode:     Continuously

Sample Drop:     Automatic

Out-Gas Power (Kw)    5.5

Out-Gas Time (Sec)    30

Purge Time (Sec)     10

Stabilization Time (Sec)    45

Integration Delay (Sec)    10

Analyse Power (Kw)    5.0

Minimum Time (Sec)    25

Maximum Time (Sec)    60

Comparator Setting    20

Accelerator / Flux Nickel Capsule + Nickel Basket (AR 508)

Graphite Crucible x1 Outer Crucible (SL 433) + x1 Inner Crucible (SL 431)

Sample Preparation Sample weight approx. 100mg. If the sample is in a powder form weigh into a nickel basket. Crimp the capsule and place inside nickel basket (AR 508).

 

Oxygen / Nitrogen in Ceramics

Power Mode:     Continuously

Sample Drop:     Automatic

Out-Gas Power (Kw)    5.5

Out-Gas Time (Sec)    30

Purge Time (Sec)     10

Stabilization Time (Sec)    45

Integration Delay (Sec)    10

Analyse Power (Kw)    5.0

Minimum Time (Sec)    25

Maximum Time (Sec)    60

Comparator Setting    20

Accelerator / Flux Nickel Capsule + Nickel Basket (AR 508)

Graphite Crucible x1 Outer Crucible (SL 433) + x1 Inner Crucible (SL 431)

Sample Preparation Sample weight approx. 100mg. If the sample is in a powder form weigh into a nickel capsule. Crimp the capsule and place inside nickel basket (AR 508).

Oxygen in Copper

Power Mode:     Continuously

Sample Drop:     Automatic

Out-Gas Power (Kw)    4.0

Out-Gas Time (Sec)    30

Purge Time (Sec)     10

Stabilization Time (Sec)    45

Integration Delay (Sec)    5

Analyse Power (Kw)    2.8

Minimum Time (Sec)    25

Maximum Time (Sec)    60

Comparator Setting    20

Accelerator / Flux None

Graphite Crucible x1 Outer Crucible (SL 433) + x1 Inner Crucible (SL 431)

Sample Preparation Sample weight approx. 1000mg. Remove any surface oxidation by abrading. Ensure the sample is clean. Wash with Acetone followed by Petroleum Spirit.

 

Oxygen in Magnesium

Power Mode:     Continuously

Sample Drop:     Automatic

Out-Gas Power (Kw)    4.0

Out-Gas Time (Sec)    30

Purge Time (Sec)     10

Stabilization Time (Sec)    45

Integration Delay (Sec)    10

Analyse Power (Kw)    2.8

Minimum Time (Sec)    25

Maximum Time (Sec)    60

Comparator Setting    20

Accelerator / Flux x2 Tin Pellets (AR 639) placed in the crucible at the start of the analysis.

Graphite Crucible x1 Outer Crucible (SL 433) + x1 Inner Crucible (SL 431)

Sample Preparation Maximum sample weight 1000mg. Clean furnace after each analysis. 

 

Oxygen / Nitrogen in Titanium

Power Mode:     Continuously

Sample Drop:     Automatic

Out-Gas Power (Kw)    6.2

Out-Gas Time (Sec)    30

Purge Time (Sec)     10

Stabilization Time (Sec)    45

Integration Delay (Sec)    10

Analyse Power (Kw)    6.0

Minimum Time (Sec)    25

Maximum Time (Sec)    60

Comparator Setting    20

Accelerator / Flux Nickel Basket Pre-Etched (AR 2344)

Graphite Crucible x1 Outer Crucible (SL 433) + x1 Inner Crucible (SL 431)

Sample Preparation Maximum sample weight 120mg.

 

Oxygen / Nitrogen in Zirconium

Power Mode:     Continuously

Sample Drop:     Automatic

Out-Gas Power (Kw)    5.8

Out-Gas Time (Sec)    30

Purge Time (Sec)     10

Stabilization Time (Sec)    45

Integration Delay (Sec)    10

Analyse Power (Kw)    5.5

Minimum Time (Sec)    25

Maximum Time (Sec)    60

Comparator Setting    20

Accelerator / Flux Nickel Basket Pre-Etched (AR 2344)

Graphite Crucible x1 Outer Crucible (SL 433) + x1 Inner Crucible (SL 431)

Sample Preparation Maximum sample weight 250mg.